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Ursodeoxycholic acid

chemical name:Ursodeoxycholic acid
appearance:white needle crystallinepowder
cas no.:128-13-2
M.W.:391.5646
M.F.:C24H39O4
assay:99%min
melting point:203-206°C
boiling point:547.148°C at 760 mmHg
package:as customers'The detailed specifications are as below:

ItemoftestingInspectionStandard
AppearanceWhiteoralmostwhitepowder,tastebitter,withoutstink.
SolubilityAlmostinsolubleinwater;solubleinmethanolandinglacialaceticacid;slightlysolubleinchloroform.
IdentificationIRspectrum:identicalwithreferencespectrum.
SpecificOpticalRotation+58°~+62°
Chloride0.02%Max
Sulfate0.05%Max
ArsenicSalt2ppmMax
BariumSaltNone
MeltingPoint200℃-204℃
LossonDrying1.0%Max
IgnitionResidue0.1%Max
HeavyMental10ppmMax
Assay(Titration)99%~101%
Particlesize95%below30цm
RelatedSubstance(TLC)
ChenodeoxycholicAcid
LithocholicAcid
CholicAcid
Unidentified
TotalImpurity
Notmorethan1.0%
Notmorethan0.1%
Notmorethan0.5%
Notmorethan0.25%
Notmorethan2.0%